Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline

S. Habil and Zuhair Jamain and Mohamad Zul Hilmey Makmud (2021) Synthesis and chemical interpretation of 4-((4-nonylphenyl) diazenyl) aniline and 4-((4-decylphenyl) diazenyl) aniline.

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Abstract

4-((4-nonylphenyl)diazenyl)aniline and 4-(4-decylphenyl)diazenyl)aniline are an azo compounds with different terminal chains. The synthesis process was started via diazotization of 4- nitroaniline with phenol formed 4-(4-nitrophenyl)phenol (1). After that, 4-(4-nitrophenyl)phenol was alkylated with 1-bromononane and 1-bromodecane to yield 1-(4-nitrophenyl)-2-(4-nonylphenyl)diazene (2) and 1-(4-decylphenyl)-2-(4-nitrophenyl)diazene (3), respectively. Finally, both molecules will undergo reduction to yield 4-((4-nonylphenyl)diazenyl)aniline (4) and 4-(4-decylphenyl)diazenyl)aniline (5), respectively. These two compounds were submitted to extensive spectroscopic examination, including Fourier Transform-Infrared (FT-IR) and Nuclear Magnetic Resonance (NMR).

Item Type:	Proceedings
Keyword:	Diazotization , Reduction , Terminal chains , FT-IR , NMR
Subjects:	Q Science > QD Chemistry > QD1-999 Chemistry
Department:	FACULTY > Faculty of Science and Natural Resources
Depositing User:	DG MASNIAH AHMAD -
Date Deposited:	31 Mar 2022 14:04
Last Modified:	31 Mar 2022 14:04
URI:	https://eprints.ums.edu.my/id/eprint/32126

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